Learning outcomes |
This UC aims to complete structural analysis methods used for the identification of organic compounds, including UV / Vis, IR, Raman, NMR, solid state NMR, and mass spectroscopic and X-ray diffraction.
At the end of UC students should know confirm the existence of chromophores by UV / Vis; acquire more data and input the same databases for new methods by IR spectroscopy to ascertain using Raman spectroscopy in the analysis of materials used in industry; namely using NMR spectroscopy for quantitative analysis; use solid NMR as a non-destructive method of analysis as medicines; know how to use mass spectrometry as a complementary method of structure determination; and to use the X-ray diffraction as a complementary method of structural characterization of the substances from their diffractograms.
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Main Bibliography |
1. Bibliografia principal - Holzgrabe, U., Diehl B., Wawer, I. “NMR Spectroscopy in Pharmaceutical Analysis” (2008), Elsevier, Netherlands - Balci, M., “Basic 1H- and 13C-NMR Spectroscopy” (2005), Elsevier, Netherlands - Anderson, R.J. et al “Organic Spectroscopic Analysis” (2004), RSC, UK 2. Bibliografia complementar - Shriner, R.L., Hermann, C.K.F., Morrill, T.C., Curtin, D.Y., “The Systematic Identification of Organic Compounds” (2004) 8th Ed.; John Wiley & Sons. - Maurer, H.H., Pfleger, K., Weber; A. A., “Mass Spectral and GC Data of Drugs, Poisons, Pesticides, Pollutants and Their Metabolites” (2011). Wiley – VCH. - Cullity, B.D., “Elements of X-ray Diffraction” (1978), 2nd Ed, Addison-Wesley, Reading, MA. - Figueiredo Gomes, C.S., “Raios X no Estudo de Materiais” (1979), Universidade de Aveiro. - Dann, S.E., “Reactions and Characterization of Solids” (2000), Royal Society of Chemistry
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