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Laboratorial Techniques in Chemistry

Code 12154
Year 2
Semester S2
ECTS Credits 6
Workload PL(45H)/TP(15H)
Scientific area Chemistry
Entry requirements -
Learning outcomes The objectives of this Course Unit focus on the development by the students of multidisciplinary projects of current interest, with the main focus on the application of laboratory techniques in Chemistry, following the principles of Green Chemistry, and, whenever possible, integrating techniques of other areas such as Physics, Biochemistry (Toxicity), Environment, with a view to the application and production of more sustainable materials.
Students should recognize the techniques they will need to develop projects proposed by the teacher, know how to apply them and adapt them in order to achieve the objectives of each project.
Syllabus 1 - Environmental Applications
1.1 - Treatment of liquid effluents
- Implementation of the installation of an electrolytic cell for the treatment of effluents with organic pollutants and monitoring of pollutant degradation

1.2 - Air quality monitoring
- Determination of the concentration of air pollutants in air samples: particulate material and chemical pollutants

2 - Metal Protection / Corrosion Inhibition
- Planning and carrying out a galvanoplasty: copper plating, zinc plating ....

3 - Polymer Chemistry
- Synthesis and colligative properties, chemical structure and properties.

4 - Green Chemistry
- Application of the principles of Green Chemistry in all the work to be developed.
Main Bibliography Atkins, P.; Jones L.; Laverman L. (2016) Chemical Principles: The Quest for Insight Seventh Edition, W. H. Freeman.
Vallero, D. (2008) Fundamentals of Air Pollution (4th Ed.), Academic Press.
Seinfeld, John H.; Pandis, Spyros N., (2006) Atmospheric Chemistry and Physics - From Air Pollution to Climate Change (2nd Ed.), John Wiley & Sons,
Roberge, P. (2006) Corrosion Basics: An Introduction, NACE International.
Rajeshwar, K.; Ibanez, J.G. (1997) Environmental Electrochemistry: Fundamentals and Applications in Pollution Abatement, Elsevier.
Stanley E. Manahan (2003) Toxicological Chemistry and Biochemistry, 3ª ed. Lewis Publishers, CRC Press LLC
Solomons G.; Fryhle C.; Snyder S A (2017) Organic Chemistry, 12.st Edition, John Wiley & Sons, New York, USA.
P Ghosh,”(2009) Polymer Science and Technology”, Mac Graw Hill, NY, 3rd edition
M. Double, A. K. Kruthiventi, (2007) "Green Chemistry and Engineering", Elsevier Science & Technology Books
Teaching Methodologies and Assessment Criteria dents will have theoretical classes where laboratory techniques that they will have to use, to carry out the proposed work and the problems associated with each work to be developed, will be addressed; it is intended that these classes have an active participation of students, through dialogue between the teacher and students.
The works must be developed in laboratory classes and a report must be made for each laboratory work carried out.
The UC Assessment will be carried out by evaluating the written reports referring to the laboratory work carried out and their discussion.
Language Portuguese. Tutorial support is available in English.
Last updated on: 2023-05-05

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