Skills Laboratory III

Code	15999
Year	2
Semester	S1
ECTS Credits	1
Workload	PL(10H)
Scientific area	Industrial Chemistry
Entry requirements	-
Learning outcomes	This course aims to provide students with practical skills that enable them to correctly and expeditiously perform basic techniques and unit operations used in Organic Chemistry. At the end of the CU students should be able to: - Properly use an extraction ampoule - Properly use a Soxhlet Extractor - Perform a liquid-liquid extraction - Perform a solid-liquid extraction - Perform a reflow - Perform distillation under reduced pressure using the rotary evaporator - Perform simple filtration - Perform vacuum filtration
Syllabus	- Liquid-liquid extraction - Solid-liquid extraction - Reflux - Distillation under reduced pressure using rotary evaporator - Simple filtration - Vacuum filtration
Main Bibliography	- J.A. Beran, “Laboratory manual for principles of general chemistry”, John W iley & Sons, 9ª ed. (2010). - J.A.M. Simões, M.A.B. Castanho, I.M.S. Lampreia, F.J.V. Santos, C.N. Castro, M.T. Pamplona, M.E.M. Piedade, “Guia do Laboratório de Química e Bioquímica”, Lidel, Lisboa (2017) - J.M. Postma, J.L. Roberts, J.L. Hollenberg, “Chemistry in the Laboratory”, W. H. Freeman and Compan y, 7ª ed. (2010). - D. T. Sawyer, W. R. Heineman, J. M. Beebe, Chemistry Experiments for Instrumental Methods, John Wiley & Sons (1984).
Language	Portuguese. Tutorial support is available in English.